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EcoSEC High Temperature GPC System

EcoSEC High Temperature System

Demanding high temperature polymer analyses, such as for polyolefins, require a system that delivers results reliably, reproducibly, and produces these results in an easy to use, safe instrument. The EcoSEC High Temperature GPC System incorporates the proven design and technology used in our ambient EcoSEC GPC System.

The dual pump system, dual flow RI detector, spacious column oven, total system temperature control, autosampler, sample prep station, safety features, and all-in-one design controlled by intuitive software combine to deliver exceptional performance.

 


The EcoSEC High Temperature GPC System features:
Reliability
Reproducibility
Stability
Safety
All-in-one design
Ease of use

 



What is unique about the EcoSEC High Temperature GPC System?
Dedicated system that is easy to use and is ready when you are »
Dual flow RI detector, delivering unparalleled RI baseline stability »
Total system temperature control, resulting in accurate flow rates and reproducible molar mass determinations with consistent results from run-to-run, day-to-day, and system-to-system »

 

 EcoSECHT_components

 



Click on the individual component links below for more detailed information
Solvent Reservoir »
Control Panel »
Temperature Controlled Pumps »
Column Oven »
Autosampler »
RI Detector »
Purge Unit and Degasser »
EcoSEC HT Workstation Software »
Column Switching Valve Option »
Sample Prep System Option »

 

 

Tosoh Bioscience can tailor a system to meet your application needs.

Does your analysis require additional detectors beyond RI?
The EcoSEC High Temperature GPC System provides easy, effortless and temperature controlled connectivity when using multi-detector configurations. We offer external light scattering and viscometry detectors, as well as coupling options for FT-IR analysis.

Contact us for a quote!

 

Instrument
Dimension 1,000 (W) × 500 (D) × 650 (H) mm 

 

Auto-injector
Injection volume  10 to 500 µL (dependent on sample loop size) 
Number of samples 24 

 

Column oven 
Temperature range  40 °C to 220 °C
Capacity  7.8 mm ID × 30 cm × 8 columns  

 

Pump 
Flow rate  0.1 to 2.0 mL/min in 0.1 mL/min steps  
Accuracy  +/- 2% 
Precision  +/- 0.2% 
Max. Pressure  15 MPA or 2,175 psi 

 

RI Detector 
Type  Bryce or dual flow type. Tungsten light source  
Cell volume  10 µL 
Noise  1.5 × 10-8 RI units (RIU) (ODCB: 1.0 mL/min, 145 ºC, response: 3 s) 
Drift 3 × 10-7 RIU/h (ODCB: 1.0 mL/min, 145 ºC)  


The EcoSEC High Temperature GPC System Workstation Software offers unparalleled versatility and includes these features:
GPC-specific EcoSEC High Temperature GPC System software to simplify system control and data handling
Controls up to 2 EcoSEC High Temperature GPC Systems
Excellent data handling and report generation
Fully featured data handling system; analyze data from two detectors
Start and stop system automatically
One license for multiple locations

 

Software features include:
Flow Diagram »
Method Templates »
Peak Editing »
Data Management »
Multiprocessing Function »
GPC Specific Quantitative Calculations »
Report Generation »

 



TSKgel polystyrene bulk calibration standards are used to calibrate GPC columns for subsequent analysis of unknown samples. The standards range from 400 to 2.1 × 107 Da.

 

 

standards_200px.jpg



TSKgel H series GPC columns are recommended for the analysis of organic-soluble polymers and are packed with spherical particles composed of polystyrene cross-linked with divinylbenzene (PS-DVB). The TSKgel HT columns are for high temperature applications (≤ 140 °C) while the TSKgel HT2 columns are used in ultra-high temperature (up to 220 °C) applications.

The figure below demonstrates the performance stability of the TSKgel GMHHR-H HT columns compared to other commercially available high temperature GPC columns during repetitive temperature changes. The TSKgel HHR HT columns and two commercially available high temperature GPC columns were subjected to drastic changes in temperature by raising the temperature for 2 hours followed by lowering the temperature for two hours for a total of 60 cycles. The number of theoretical plates was shown to remain constant for the TSKgel HHR HT columns and to decrease by 15% for the two commercially available high temperature GPC columns; thus revealing the superior performance stability of the TSKgel HHR HT columns.

 

 

Column Durability

Column_durability.png 
Column:          TSKgel GMHHR-H HT2, 5 µm, 7.8 mm ID × 30 cm × 2
Mobile Phase: ODCB with 0.05% BHT
Flow rate:       1.0 mL/min
Detection:       RI (EcoSEC High Temperature GPC System)
Temperature: 40 to 145°C